Data were collected using a Bruker APEX-II CCD diffractometer equipped with an Oxford Cryosystems low-temperature apparatus operating at T = 100(2) K.ĭata were measured using f and w scans scans of 1 ° per frame for 30 s using MoK a radiation (fine-focus sealed tube, 45 kV, 35 mA). A green prism-shaped crystal with dimensions 0.48×0.39×0.23 mm was mounted on a loop with paratone oil. ![]() The final wR 2 was 0.1163 (all data) and R 1 was 0.0414 (I > 2(I)).Įxperimental Extended. ![]() The structure was refined with version of ShelXL-97 (Sheldrick, 2008) using Least Squares minimisation.Ĭrystal Data. The structure was solved with the XT (Sheldrick, 2015) structure solution program, using direct and dual-space solution methods and by using Olex2 (Dolomanov et al., 2009), as the graphical interface. The crystal was cooled to T = 100(2) K during data collection. ![]() ![]() A suitable crystal (0.48×0.39×0.23 mm) was selected and mounted on a loop with paratone oil on a Bruker APEX-II CCD diffractometer. Single green prism-shaped crystals of ( NS06252015A) were recrystallised from a mixture of diethyl ether and acetonitrile by vapour diffusion.
0 Comments
Leave a Reply. |
AuthorWrite something about yourself. No need to be fancy, just an overview. ArchivesCategories |